X-CT引导的矿物赋存状态及微区表征研究
投稿时间:2022-07-10  修订日期:2023-08-10  点此下载全文
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作者单位邮编
李伯平 核工业北京地质研究院 100029
李黎 核工业北京地质研究院 
王娅楠 核工业北京地质研究院 
刘瑞萍 核工业北京地质研究院 
郭冬发 核工业北京地质研究院 
中文摘要:在常规岩矿鉴定过程中普遍存在对岩芯内部构造、矿物分布等缺乏了解的问题。X-CT技术作为一种无损分析测试手段,近年来在地球科学领域越来越受到关注。文章以相山火山岩型和沙特碱性花岗岩型岩芯样品为研究对象,采用高分辨微焦X射线断层扫描(X-CT)技术对岩芯中高密度矿物的形貌、空间分布等参数进行表征。通过对X-CT测定数据的解析,可以快速准确地获得目标重矿物在岩芯中的空间位置。依据X-CT给出的目标矿物所在岩芯中空间相对位置,引导传统制靶工艺制备目标区域的靶样,联用电子扫描电镜(SEM)和激光烧蚀电感耦合等离子体质谱(LA-ICP-MS)进行微区表征,获得了岩芯中稀土矿物和含铀矿物的空间赋存状态以及微区特定元素分布信息。由于预先采用X-CT对目标矿物及对应微区进行空间位置标定,使得制靶效率和选点准确度得到有效提高。
中文关键词:X射线  数字成像  灰度  矿物纯度
 
Study on Mineral Occurrence and Micro Region Characterization Guided by X-CT Gray Scale Imaging
Abstract:In the process of conventional rock and ore identification, there is a general lack of understanding of the internal structure and mineral distribution of the core,just like a “Blind box”. As a non-destructive 3D imaging and analysis technique, high-resolution X-ray computed tomography (HRXCT) had been widely used in geology science. Because heavy minerals have strong attenuation on X-rays, they can be effectively digitally separated from common non-metallic minerals, so as to obtain the spatial occurrence state of heavy minerals in the core, therefore, X-CT can provide technical support for digital core. This paper takes the core samples of Xiangshan volcanic rock type and Saudi Arabia alkaline granite type as the research object, and uses high-resolution micro-focus X-ray tomography (X-CT) technology to characterize the morphology, spatial distribution and other parameters of high-density minerals in the core. The spatial position of the target heavy mineral in the core can be quickly and accurately obtained by analyzing the X-CT data. According to the relative spatial position of the target minerals in the core given by X-CT, guide the traditional target preparation process to prepare the target samples in the target area, and use the combination of electronic scanning electron microscopy (SEM) and laser ablation inductively coupled plasma mass spectrometry (LA-ICP-MS) for micro-area characterization to obtain the spatial occurrence status of REE minerals and uranium-bearing minerals in the core and the distribution information of specific elements in the interesting area. Due to the pre-use of X-CT to locating the spatial position of the target minerals and corresponding micro-area, the efficiency of target preparation and the accuracy of point selection have been effectively improved.
keywords:X-CT guide  Gray value  Heavy minerals  spatial occurrence
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